Crystallosolvate Formation in Copper(II) 4-Nitrobenzoate Complex Systems
Institute of Inorganic Chemistry, Technology and Materials, Faculty of Chemical and Food Technology STU, Radlinského 9, 812 37 Bratislava
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Abstract: Three different products [Cu2(4-NO2bz)4(denia)]∙(TOL) (1), [Cu2(4-NO2bz)4(EtOH)2] (2), and [Cu2(4-NO2bz)4(H2O)(AC)] (3) were obtained by the reaction of copper(II) acetate, N,N-diethylnicotinamide and 4-nitrobenzoic acid in different solvents. Complexes under study were characterized by elemental analysis and by IR, EPR or UV/VIS spectra. X-ray powder diffraction pattern were obtained to characterize samples and to compare obtained products with known ones.
Keywords: copper complexes, diethylnicotinamide, 4-nitrobenzoate, crystallosolvate
Full paper in Portable Document Format: acs_0059.pdf
Acta Chimica Slovaca, Vol. 3, No. 1, 2010, pp. 73—80